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Ugi Three-Component Coupling Strategy for the Synthesis of Bridged Bicyclic Iminosugars
A novel and catalyst-free approach has been accomplished for the synthesis of bridged bicyclic iminosugars through a Ugi 3...
Organic & Biomolecular Chemistry
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A green and cascade synthesis of functionalized 2-sec.amino-thiophenes from ketene dithioacetals
We have reported the synthesis of pharmacologically valuable tetrasubstituted 2-aminothiophenes through a multi-component ...
Organic & Biomolecular Chemistry
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Recent advances in visible-light-driven photocatalytic synthesis of biologically active N-heterocycles
Heterocycles that contain nitrogen are a very significant class of chemicals that are employed extensively in medicinal ch...
Organic & Biomolecular Chemistry
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Iron Catalysis Enables Mild C–Se Bond Formation via Decarboxylative Selenylation
Selenium-containing compounds are pivotal in bioactive molecules, yet efficient C–Se bond formation is of significant inte...
Organic & Biomolecular Chemistry
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Phenoxysulfonyl Azide: A New Diazo-transfer Reagent for Metal–Free Conversion of Amines to Azides
Phenoxysulfonyl azide (PSA, 1) was synthesized from 1,1'-sulfonylbis(2-methyl-1H-imidazole) (2) and studied for its di...
Organic & Biomolecular Chemistry
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Base-Promoted Tandem Synthesis of Nitrogen-Containing Compounds: MN(SiMe₃)₂ as Potential Nitrogen Sources
The metal-silylamides [MN(SiMe₃)₂, M = Li, Na, and K] are widely used Brønsted bases and have become among the most p...
Organic & Biomolecular Chemistry
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Molybdenum Catalyzed Acceptorless Dehydrogenative Approach for Quinoline Synthesis Using Amino Alcohol
We report here bidentate phosphine-ligand based molybdenum π-allyl complex [Mo(CO)2(η3-C3H5)(DPPE)Cl] (Mo-1; DPPE =) in th...
Organic & Biomolecular Chemistry
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Synthesis and Evaluation of Naphthoquinone-based Probes for Activity-based Protein Profiling of Oxidoreductases
Activity-based protein profiling (ABPP) has become a highly valuable proteomic technique over the past decades especially ...
Organic & Biomolecular Chemistry
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Silver-Catalyzed Synthesis of Polyfunctionalized 1,7- and 2,7- Benzonaphthyridine Scaffolds and their Access to Perlolidine Derivatives
A regio- and chemoselective silver-catalyzed one-pot synthesis of benzo[b][1,7]- and benzo[c][2,7]-naphthyridines has been...
Organic & Biomolecular Chemistry
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Co(III)-catalyzed allylation reaction of 2-alkenylpyridines with 2-vinylaziridines: access to 1,4-dienes
A Cp*(CO)CoI2-catalyzed C–H allylation of 2-alkenylpyridines with 2-vinylaziridines is described. This method provides an ...
Organic & Biomolecular Chemistry
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Pyreno-1,2,4-Triazines as Multifunctional Luminogenic Click Reagents
Several examples of 1,2,4-triazines that contain a pyrene fragment attached to the C5 position and a carbonyl functional g...
Organic & Biomolecular Chemistry
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Chimeric enediyne for targeted degradation of tumor-associated protein
Protein-radical-oxidation targeting enediyne chimera (PROTEC) comprising an enediyne warhead and a protein-targeting moiet...
Organic & Biomolecular Chemistry
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Transition-metal and Photocatalyst-free Oxidative Cleavage of Aryl alkynes with PIDA/Iminoiodinanes in Visible Light
We report a transition-metal and photocatalyst-free method for the oxidative cleavage of aryl alkynes using phenyliodine d...
Organic & Biomolecular Chemistry
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Tumor-targeted fluorescent probes for the detection of hNQO1 in cancer cells
Fluorescent probes for single analyte might produce 'false-positive' signals because the levels of the biomarkers ...
Organic & Biomolecular Chemistry
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Synthesis of naphth[2,1-a]azulenes via [8 + 2] cycloaddition of 2Hcyclohepta[b]furan-2-ones, and their reactivity, optical, and structural properties
A concise and efficient synthetic route to naphth[2,1-a]azulenes was developed via [8 + 2] cycloaddition of 2Hcyclohepta[b...
Organic & Biomolecular Chemistry
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Selective Electrochemical Trifluoromethylation of Arylamide-or Aryl-substituted Pyrrole Derivatives †
A selective electrochemical trifluoromethylation reaction for pyrroles, particularly those containing additional aryl grou...
Organic & Biomolecular Chemistry
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Stereoselective synthesis of a KRASG12C inhibitor with quinoline-piperazine scaffold
We developed a novel synthetic route for the KRASG12C inhibitor, focusing on the efficient construc-tion of its central qu...
Organic & Biomolecular Chemistry
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PIDA-Mediated Synthesis of Kynurenine Derivatives by Oxidative Fragmentation of Tryptophan Scaffold
Kynurenine metabolite is derived from aromatic amino acid tryptophan and its chemical synthesis has been sought for unders...
Organic & Biomolecular Chemistry
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Synthesis and stability of collagen mimetic peptides featuring δ-heteroatom-substituted prolines
We describe the first investigation of collagen mimetic peptides harboring proline surrogates with heteroatoms at the δ-po...
Organic & Biomolecular Chemistry
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A MnCl2 Catalyzed Synthesis of Aldehydes from Organohalides by Using Samarium Metal in DMF
Catalyzed by MnCl2, a novel coupling reaction between organohalides and N,N-dimethylformamide (DMF) was investigated in th...
Organic & Biomolecular Chemistry
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Artemselenoids A−H, eight guaiane-type sesquiterpenoid dimers from Artemisia selengensis and their antihepatoma activities
Eight undescribed guaiane-type sesquiterpenoid dimers (GSDs), artemselenoids A−H (1−8), together with nine known GSDs (9−1...
Organic & Biomolecular Chemistry
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Phosphinylation/Cyclization of Propynolaldehydes to Isobenzo- furanylic Phosphine Oxides Displaying AIE Properties
Investigating organic reactions to synthesize novel molecules that exhibit aggregation-induced emission (AIE) characterist...
Organic & Biomolecular Chemistry
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Energy Transfer Mediated Carbonylimination of Alkenes Using Bifunctional Reagent
A photoinduced EnT-mediated generation of acyl radicals has been accomplished using rationally designed acyl oxime ethers ...
Organic & Biomolecular Chemistry
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Total Synthesis of (±)-Halichonine B
The stereocontrolled total synthesis of (±)-halichonine B was achieved in 18 steps for the longest linear sequence. T...
Organic & Biomolecular Chemistry
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Brønsted Acid-Catalyzed Synthesis of Sulfinamidines and Sulfinimidate Esters through Electrophilic Fluorination and Substitution
In this work, we present an innovative Brønsted acid-catalyzed approach for the concurrent preparation of sulfinamidi...
Organic & Biomolecular Chemistry
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A β-Hairpin Peptide Derived from Aβ Forms Different Oligomers in the Crystal State and in Aqueous Solution
The supramolecular assembly of amyloid β into soluble oligomers is critical Alzheimer’s disease (AD) progression. Soluble ...
Organic & Biomolecular Chemistry
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Computational Exploration of Vinyl Sulfoxonium Ylide Chemistry
This review comprehensively examines the computational techniques employed to elucidate the reactivity, selectivity, and m...
Organic & Biomolecular Chemistry
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Selenium-catalyzed Allylic C-H Phosphoramidation of Alkenes
We report herein a synthesis of allylic phosphoramidates from alkenes by selenium-catalyzed allylic C-H derivatization. Th...
Organic & Biomolecular Chemistry
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Total synthesis and structure–antifouling activity relationship of scabrolide F
An efficient synthetic strategy for scabrolide F (7), a norcembranolide diterpene that was isolated from the Taiwanese sof...
Organic & Biomolecular Chemistry
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Synthesis, characterization and photophysical studies of dual emissive base-modified fluorescent nucleosides
A straightforward and efficient methodology has been employed for the synthesis of a diverse set of base-modified fluoresc...
Organic & Biomolecular Chemistry
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