Rapid and Sensitive Determination of Alkynyl Steroid Hormones in Milk Samples Using Magnetic Solid-Phase Extraction Coupling Click Derivatization-Based LC–MS Method

Ma L, Yates SR. A review on structural elucidation of metabolites of environmental steroid hormones via liquid chromatography–mass spectrometry. TrAC Trends Anal Chem. 2018;109:142–53.

Article  CAS  Google Scholar 

Ojoghoro JO, Scrimshaw MD, Sumpter JP. Steroid hormones in the aquatic environment. Sci Total Environ. 2021;792: 148306.

Article  CAS  PubMed  Google Scholar 

Xu X, Liang F, Shi J, Zhao X, Liu Z, Wu L, Song Y, Zhang H, Wang Z. Determination of hormones in milk by hollow fiber-based stirring extraction bar liquid–liquid microextraction gas chromatography mass spectrometry. Anal Chim Acta. 2013;790:39–46.

Article  CAS  PubMed  Google Scholar 

Zhu W, Peng H, Luo M, Yu N, Xiong H, Wang R, Li Y. Zipper-like magnetic molecularly imprinted microspheres for on/off-switchable recognition and extraction of 17β-estradiol from food samples. Food Chem. 2018;261:87–95.

Article  CAS  PubMed  Google Scholar 

Jouan PN, Pouliot Y, Gauthier SF, Laforest JP. Hormones in bovine milk and milk products: a survey. Int Dairy J. 2006;16(11):1408–14.

Article  CAS  Google Scholar 

Trabert B, Sherman ME, Kannan N, Stanczyk FZ. Progesterone and breast cancer. Endocr Rev. 2020;41(2):320–44.

Article  PubMed  Google Scholar 

Plotan M, Elliott CT, Frizzell C, Connolly L. Estrogenic endocrine disruptors present in sports supplements. A risk assessment for human health. Food Chem. 2014;159(1):157–65.

Article  CAS  PubMed  Google Scholar 

Servos MR, Bennie DT, Burnison BK, Jurkovic A, McInnis R, Neheli T, Schnell A, Seto P, Smyth SA, Ternes TA. Distribution of estrogens, 17β-estradiol and estrone, in Canadian municipal wastewater treatment plants. Sci Total Environ. 2005;336(1):155–70.

Article  CAS  PubMed  Google Scholar 

López-García M, Romero-González R, Garrido FA. Determination of steroid hormones and their metabolite in several types of meat samples by ultra high performance liquid chromatography—Orbitrap high resolution mass spectrometry. J Chromatogr A. 2018;1540:21–30.

Article  PubMed  Google Scholar 

Xiong X, Li D, Du Z, Xiong C, Jiang H. Magnetic solid-phase extraction modified quick, easy, cheap, effective, rugged and safe method combined with pre-column derivatization and ultra-high performance liquid chromatography-tandem mass spectrometry for determination of estrogens and estrogen mimics in pork and chicken samples. J Chromatogr A. 2020;1622:461137.

Article  CAS  PubMed  Google Scholar 

Wang S, Geng Y, Sun X, Wang R, Zheng Z, Hou S, Wang X, Ji W. Molecularly imprinted polymers prepared from a single cross-linking functional monomer for solid-phase microextraction of estrogens from milk. J Chromatogr A. 2020;1627:461400.

Article  CAS  PubMed  Google Scholar 

Decheng S, Xia F, Zhiming X, Shulin W, Shi W, Peilong W. Trace analysis of progesterone and 21 progestins in milk by ultra-performance liquid chromatography coupled with high-field quadrupole-orbitrap high-resolution mass spectrometry. Food Chem. 2021. https://doi.org/10.1016/j.foodchem.2021.130115.

Article  PubMed  Google Scholar 

Yu Y, Kuang M, Zheng B, Wang M, Liu Z, Xu H, Wang J. Detection of multiple endocrine-disrupting chemicals in milk: Improved and safe high performance liquid chromatography tandem mass spectrometry method. J Sep Sci. 2022;45(9):1538–49.

Article  CAS  PubMed  Google Scholar 

Anari MR, Bakhtiar R, Zhu B, Huskey S, Franklin RB, Evans DC. Derivatization of ethinylestradiol with dansyl chloride to enhance electrospray ionization: application in trace analysis of ethinylestradiol in Rhesus monkey plasma. Anal Chem. 2002;74(16):4136–44.

Article  CAS  PubMed  Google Scholar 

Fu XK, Han SQ, Ha W, Shi YP. Click chemoselective probe with a photoswitchable handle for highly sensitive determination of steroid hormones in food samples. J Agr Food Chem. 2023;71(40):14814–24.

Article  CAS  Google Scholar 

Li Q, Liu J, Zhang L, Shi Y, Li G. Click isotope mass probe for highly selective determination of trace steroid hormones in food samples. J Agr Food Chem. 2022;70(18):5748–55.

Article  CAS  Google Scholar 

Suazo KF, Park KY, Distefano MD. A not-so-ancient grease history: Click chemistry and protein lipid modifications. Chem Rev. 2021;121(12):7178–248.

Article  CAS  PubMed  PubMed Central  Google Scholar 

Wan Ibrahim WA, Nodeh HR, Aboul-Enein HY, Sanagi MM. Magnetic solid-phase extraction based on modified ferum oxides for enrichment, preconcentration, and isolation of pesticides and selected pollutants. Crit Rev Anal Chem. 2015;45(3):270–87.

Article  CAS  PubMed  Google Scholar 

Wierucka M, Biziuk M. Application of magnetic nanoparticles for magnetic solid-phase extraction in preparing biological, environmental and food samples. TrAC Trends Anal Chem. 2014;59:50–8.

Article  CAS  Google Scholar 

Gao Q, Luo D, Bai M, Chen Z-W, Feng YQ. Rapid determination of estrogens in milk samples based on magnetite nanoparticles/polypyrrole magnetic solid-phase extraction coupled with liquid chromatography–tandem mass spectrometry. J Agr Food Chem. 2011;59(16):8543–9.

Article  CAS  Google Scholar 

Jiao Z, Zhang Y, Fan H. Ultrasonic-microwave method in preparation of polypyrrole-coated magnetic particles for vitamin D extraction in milk. J Chromatogr A. 2016;1457:7–13.

Article  CAS  PubMed  Google Scholar 

Xu SN, Zhao Q, He HB, Yuan BF, Feng YQ, Yu QW. Rapid determination of polycyclic aromatic hydrocarbons in environmental water based on magnetite nanoparticles/polypyrrole magnetic solid-phase extraction. Anal Methods. 2014;6(17):7046–53.

Article  CAS  Google Scholar 

Hu YN, Zhan JT, Bai PR, An N, Tan JJ, Wang YZ, Zhu QF, Feng YQ. In-depth profiling of di(2-ethylhexyl) phthalate metabolic footprints in rats using click chemistry-mass spectrometry probes. J Hazard Mater. 2023;452:131190.

Article  CAS  PubMed  Google Scholar 

Li Q, Li G, Fan L, Yu Y, Liu J. Click reaction triggered turn-on fluorescence strategy for highly sensitive and selective determination of steroid hormones in food samples. Food Chem. 2022;374: 131565.

Article  CAS  PubMed  Google Scholar 

Razmkhah K, Sereshti H, Soltani S, Nodeh HR. Extraction and determination of three steroid molecules in milk using functionalized magnetic carbon nanotube-based solid phase extraction coupled with HPLC. Food Anal Methods. 2018;11(11):3179–89.

Article  Google Scholar 

Comments (0)

No login
gif